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Which technique is best suited for determining the crystal structure of a solid compound?
- IR Spectroscopy
- NMR Spectroscopy
- X-ray Diffraction
- Mass Spectrometry
Answer: X-ray Diffraction
XRD analyzes diffraction patterns of X-rays scattered by crystal lattice, revealing atomic arrangement, unit cell parameters, phase identification. Fundamental for materials characterization. [[NCERT Chemistry Class 12]]